Solvents and Reagents

Intro ABI Expedite Biosearch 8000 Cyclone MerMade PolyPlex Beckman Oligo Pharmacia UltraMild Supports Reagents

5'-3' Synthesis Me-Phosphonamidite Me-Phosphoramidite H-Phosphonate Sulfurization ODM

Duplex Stabilization PCR/Sequencing Structural

UltraMILD Terminus Sequence 3'-Modifiers CPR Spacers Dendrimers Photocleavable OPeC

Dabcyl Biotin Fluorescein Rhodamine Cyanine Acridine DNP Cholesterol Psoralen EDTA

TOM RNA Amidites TOM RNA Supports inor Base TOM RNA RNA Amidites RNA Supports Minor Base RNA 2'-OMe-RNA 2'-OMe-Supports Minor 2'-OMe 2'-F-RNA 2'-Se-Me-RNA

ABI Expedite Biosearch 8000 Cyclone Mermade Polyplex Beckman Pharmacia/Amersham UltraMild Alternatives H-Phosphonates Sulfurizing Complete List

NAIM Triphosphates Purification Miscellaneous Physical Properties Index General ;Information

Symbols-A A-C C-D D-G G-I I-P P-T T T-Z Updates

Glen Research offers a full line of solvents and reagents in suitable bottles and formulations for use on various DNA synthesizers. All solvents and reagents are prepared to our exacting specifications to ensure the highest coupling efficiencies and are passed through a 0.2 micron filter during packaging to eliminate particulate contamination. Glen Research offers the activators below in powder form for later dissolution in anhydrous acetonitrile or as a prepared solution.

Item	Catalog No.	Pack	Price ($)
Activator
Sublimed 1H-Tetrazole in Anhydrous Acetonitrile	30-3100-45	45mL	40.00
	30-3100-52	200mL	100.00
	30-3100-57	450mL	200.00
	30-3100-62	2000mL	760.00
	30-3102-52	200mL	100.00
	30-3102-66	60mL	50.00
0.40M Tetrazole in Acetonitrile	30-3105-71	1000mL	225.00
1H-Tetrazole in Anhydrous Acetonitrile	30-3110-51	150mL	60.00
	30-3110-57	450mL	150.00
	30-3110-62	2000mL	500.00
	30-3112-52	200mL	65.00
5-Ethylthio-1H-tetrazole (Dissolve 1g in 31mL anhydrous acetonitrilefor a 0.25M solution)	30-3040-10	1g	35.00
	30-3040-20	2g	60.00
	30-3040-25	25g	500.00
0.25M 5-Ethylthio-1H-Tetrazole in Anhydrous Acetonitrile	30-3140-45	45mL	40.00
	30-3140-52	200mL	100.00
	30-3140-57	450mL	200.00
	30-3140-61	960mL	365.00
	30-3140-62	2000mL	760.00
	30-3142-52	200mL	100.00
	30-3142-66	60mL	50.00
4,5-Dicyanoimidazole (DCI), crystalline (Dissolve 1g in 34mL anhydrous acetonitrile	30-3050-10	1g	35.00
	30-3050-25	25g	500.00
0.25M DCI in Anhydrous Acetonitrile	30-3150-45	45mL	40.00
	30-3150-52	200mL	100.00
	30-3150-57	450mL	200.00
	30-3150-61	960mL	365.00
	30-3150-62	2000mL	760.00
	30-3152-52	200mL	100.00
	30-3152-66	60mL	50.00
5-Benzylthio-1H-tetrazole (Dissolve 1g in 21.3mL anhydrous acetonitrile for a 0.25M solution)	30-3070-10	1g	35.00
	30-3070-20	2g	60.00
	30-3070-25	25g	500.00
0.25M 5-Benzylthio-1H-tetrazole in Acetonitirle	30-3170-45	45mL	40.00
	30-3170-52	200mL	100.00
	30-3170-57	450mL	200.00
	30-3170-62	2000mL	760.00
	30-3172-52	200mL	100.00
	30-3172-66	60mL	50.00
Diluent
Acetonitrile, anhydrous	40-4050-45	60mL	12.00
	40-4050-50	100mL	16.00
	40-4050-53	300mL	40.00
	40-4050-57	450mL	50.00
Cap Mix A
Tetrahydrofuran/ 2,6-Lutidine/ Acetic Anhydride	40-4010-45	45mL	16.00
	40-4010-52	200mL	30.00
	40-4010-57	450mL	72.00
	40-4010-61	960mL	154.00
	40-4010-62	2000mL	325.00
Tetrahydrofuran/ Acetic Anhydride	40-4012-50	100mL	20.00
	40-4012-52	200mL	30.00
	40-4012-57	450mL	72.00
	40-4012-62	2000mL	275.00
	40-4012-66	60mL	15.00
Acetonitrile/MeIm	40-4015-71	1000mL	145.00
Tetrahydrofuran/ Pyridine/ Acetic Anhydride	40-4110-45	45mL	16.00
	40-4110-52	200mL	30.00
	40-4110-57	450mL	72.00
	40-4110-62	2000mL	325.00
UltraMild Capping Reagents
5% Phenoxyacetic anhydride in THF/Pyridine	40-4210-52	200mL	120.00
	40-4210-57	450mL	260.00
5% Phenoxyacetic anhydride in THF	40-4212-52	200mL	115.00
	40-4212-57	450mL	250.00
Cap Mix B
6.5% Dimethylaminopyridine in Tetrahydrofuran	40-4020-45	45mL	16.00
	40-4020-52	200mL	30.00
Cap Mix B1: Acetonitrile/Ac2O	40-4026-75	500mL
Cap Mix B2: Acetonitrile/Lutidine	40-4027-75	500mL
Cap Mix B1 + Cap Mix B2		1000mL	160.00
10% 1-Methylimidazole in Tetrahydrofuran	40-4120-45	45mL	16.00
	40-4120-52	200mL	30.00
	40-4120-57	450mL	72.00
	40-4120-62	2000mL	325.00
10% 1-Methylimidazole in Tetrahydrofuran/Pyridine	40-4122-51	150mL	30.00
	40-4122-52	200mL	40.00
	40-4122-57	450mL	96.00
	40-4122-62	2000mL	325.00
	40-4122-66	60mL	20.00
16% 1-Methylimidazole in Tetrahydrofuran	40-4220-45	45mL	20.00
	40-4220-52	200mL	40.00
	40-4220-57	450mL	96.00
	40-4220-61	960mL	204.00
	40-4220-62	2000mL	425.00
UniCap
UniCap Phosphoramidite	10-4410-02	0.25g	50.00
	10-4410-05	0.5g	100.00
	10-4410-10	1.0g	200.00
	10-4410-20	2.0g	400.00
Oxiudizing Solution
0.05M I2 in Pyridine/H2O	40-4035-71	1000mL	160.00
0.05M Iodine in Tetrahydrofuran/ Water/ Pyridine	40-4130-55	240mL	36.00
	40-4130-57	450mL	72.00
	40-4130-62	2000mL	325.00
0.02M Iodine in Tetrahydrofuran/ Water/ Pyridine	40-4132-52	200mL	40.00
	40-4132-55	240mL	48.00
	40-4132-57	450mL	96.00
	40-4132-62	2000mL	325.00
	40-4132-66	60mL	20.00
0.10M Iodine in Tetrahydrofuran/ Pyridine/ Water	40-4230-52	200mL	30.00
	40-4230-57	450mL	72.00
	40-4230-61	960mL	154.00
	40-4230-62	2000mL	325.00
0.02M Iodine in Tetrahydrofuran/Pyridine/Water	40-4330-52	200mL	30.00
	40-4330-57	450mL	72.00
	40-4330-61	960mL	154.00
	40-4330-62	2000mL	325.00
3% Iodine in Tetrahydrofuran/Pyridine/Water	40-4430-52	200mL	30.00
Sulfurizing
Sulfurizing Reagent	40-4036-10	1g	50.00
	40-4036-20	2g	100.00
Silanized Bottle (one bottle at no charge when ordered with Sulfurizing Reagent)
ABI (240mL capacity)	40-4036-A1	each	10.00
ABI (450mL capacity)	40-4036-A2	each	10.00
Biosearch 8000 (100mL capacity)	40-4036-C1	each	10.00
Biosearch 8000 (500mL capacity)	40-4036-C2	each	10.00
Expedite 8905 (150mL capacity)	40-4036-C3	each	10.00
Expedite 8909 and Cyclone (240mL capacity)	40-4036-C4	each	10.00
Beckman Oligo 1000 (30mL capacity)	40-4036-B1	each	10.00
Sulfurizing Reagent II (DDTT) (Dissolve at a concentration of 1g/100mL to form an approximate 0.05M solution)	40-4037-10	1g	50.00
	40-4037-20	2g	100.00
0.05M Sulfurizing Reagent II in pyridine/acetonitrile	40-4137-51	100ml	100.00
	40-4137-52	200mL	200.00
	40-4137-57	450mL	450.00
Deblocking Mix
3% Dichloroacetic acid in Dichloromethane	40-4040-57	450mL	36.00
	40-4040-62	2000mL	144.00
	40-4040-71	1000mL	95.00
2.5% Dichloroacetic acid in Dichloromethane	40-4042-57	450mL	36.00
	40-4042-62	2000mL	144.00
Dichloroacetic acid (DCA)	40-4044-50	100mL	50.00
	40-4044-54	120mL	60.00
DCM	40-4100-62	2000mL	120.00
3% TCA/DCM	40-4140-57	450mL	36.00
	40-4140-61	960mL	75.00
	40-4140-62	2000mL	144.00
	40-4140-68	180mL	18.00
	40-4140-69	900mL	80.00
H-Phosphonate Reagents
Activator for monomers and capping reagent
1-Adamantanecarbonyl chloride is available from Aldrich, Catalog No. 117722.
Diluent
Acetonitrile/Pyridine (50:50), anhydrous	40-4550-50	100mL	24.00
Acetonitrile/Pyridine (95:5), anhydrous	40-4551-50	100mL	24.00
Capping Reagent
Isopropyl Phosphite/Acetonitrile/Pyridine	40-4510-45	45mL	36.00
Neutralizer
Acetonitrile/Pyridine	40-4500-51	150mL	28.00
Wash Solvent
Acetonitrile/Pyridine	40-4500-60	960mL	90.00
Oxidizing Solution (*Both reagents are required for oxidation of H-phosphonate linkages)
I₂ in Pyridine/H₂O/THF*	40-4531-45	45mL	12.00
THF/H₂O/TEA*	40-4532-45	45mL	12.00
Poly-Pak Purification Reagents
Wash Solvent Kit (Sufficient for use with up to 10 Poly-Pak cartridges)	60-4900-01	each	60.00
2.0M Triethylamine Acetate (TEAA)	60-4110-52	200mL	60.00
HPLC Grade	60-4110-57	450mL	120.00
	60-4110-60	960mL	200.00
	60-4110-62	2L	400.00
2% Aqueous Trifluoroacetic Acid	60-4040-57	450mL	36.00
3% Aqueous Trifluoroacetic Acid	60-4041-57	450mL	36.00
4% Aqueous Trifluoroacetic Acid	60-4042-57	450mL	36.00
UltraMild Reagents
Cap Mix A
5% Phenoxyacetic anhydride in THF/Pyridine	40-4210-52	200mL	120.00
	40-4210-57	450mL	260.00
5% Phenoxyacetic anhydride in THF	40-4212-52	200mL	115.00
	40-4212-57	450mL	250.00
Deprotection Solution
0.05M Potassium Carbonate in Methanol	60-4600-30	30mL	30.00

Please contact Glen Research if you have any questions or comments!