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BIOSEARCH 8000 SERIES

STERLING CE PHOSPHORAMIDITES

Glen Research CE (ß-cyanoethyl) Phosphoramidites are produced and packaged to ensure the highest performance on DNA synthesizers. Every Glen Research product is accompanied by a Certificate of Analysis and HPLC trace, showing the results of our QC testing. Every Glen Research monomer vial is specially cleaned to eliminate particulate contamination

ItemCatalog No.PackPrice ($)
10-1000-02 0.25g 12.50
  10-1000-05 0.5g 25.00
  10-1000-10 1.0g 50.00
  10-1000-20 2.0g 100.00
  10-1000-50 5.0g 250.00
10-1010-02 0.25g 12.50
  10-1010-05 0.5g 25.00
  10-1010-10 1.0g 50.00
  10-1010-20 2.0g 100.00
  10-1010-50 5.0g 250.00
10-1015-02 0.25g 12.50
  10-1015-05 0.5g 25.00
  10-1015-10 1.0g 50.00
  10-1015-20 2.0g 100.00
  10-1015-50 5.0g 250.00
10-1020-02 0.25g 12.50
  10-1020-05 0.5g 25.00
  10-1020-10 1.0g 50.00
  10-1020-20 2.0g 100.00
  10-1020-50 5.0g 250.00
10-1029-02 0.25g 12.50
  10-1029-05 0.5g 25.00
  10-1029-10 1.0g 50.00
  10-1029-20 2.0g 100.00
  10-1029-50 5.0g 250.00
10-1030-02 0.25g 12.50
  10-1030-05 0.5g 25.00
  10-1030-10 1.0g 50.00
  10-1030-20 2.0g 100.00
  10-1030-50 5.0g 250.00

QUALITY ASSURANCE

Every batch of these CE Phosphoramidites is tested as follows

  1. HPLC
    a) Identity is confirmed by comparison with a reference sample.
    b) Purity is determined by HPLC to be ≥98.0%.
  2. TLC
    Purity is verified by TLC.
  3. 31P NMR
    Purity is determined by 31P NMR to be ≥98%.
  4. Coupling Test
    Coupling efficiency is determined to be ≥99%.
  5. Solution Test
    A 0.1M solution is determined to be clear and free of particulate contamination.
  6. Loss on Drying
    Volatile contaminants are determined to be ≤2%.

STERLING SOLVENTS/REAGENTS

All solvents and reagents are prepared to our exacting specifications to ensure the highest synthesis efficiency and are passed through a 0.2 micron filter during packaging to eliminate particulate contamination.

Item Catalog No.PackPrice ($)
Activator
30-3110-51 150mL Discontinued
  30-3110-57 450mL Discontinued
  30-3110-62 2L Discontinued
Diluent
40-4050-45 60mL 12.00
  40-4050-50 100mL 16.00
Cap Mix A
40-4012-62 2L 275.00
Cap Mix B
40-4122-62 2L 325.00
Oxidizing Solution
40-4132-62 2L 325.00
Deblocking Mix
40-4042-57 450mL 36.00
  40-4042-62 2L 144.00
40-4044-50 100mL 50.00

ABBREVIATIONS

Ac2O = Acetic Anhydride
CE = Cyanoethyl
CPG = Controlled Pore Glass
DCA = Dichloroacetic Acid
DCM = Dichloromethane
I2 = Iodine
MeIm = 1-Methylimidazole
THF = Tetrahydrofuran

See also

Alternative Solvents p31

Supports and Columns p10-11

http://www.glenres.com/Catalog/biosearch8000.html

 
Please contact Glen Research if you have any questions or comments!
 
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